Цены ВОЙТИ РЕГИСТРАЦИЯ

Категории: Все - synthesis - purification - reduction

по Tony Zoltika 18 лет назад

252

Rearrangements

The text covers various chemical processes and methodologies focusing on the transformation and purification of organic compounds. It details the reduction of ketones and the use of LDA in synthesis and rearrangement processes.

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Reduction of ketone

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- cyclization of carboxylic acid to cyclic ketone

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- rearrangement

- synthesis of Grignard-reagent

- treatment with Grignard-reagent of aldehyde

- cyclization of product to alkyl-laktone

- reduction of aldehyde with NaBH4

- cyclization of second OH to lactone

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- acylation and purification

- LDA synthesis and actual rearrangement

- purification

- cyclization of (alkyl) carboxylic acid to alkylated cyclic ketone

ester hydrolysis